ABSTRACT

Background of the Process . . . . . . . . . . . . . . . . . . . 223

Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 224

Brief Description of the Drawing . . . . . . . . . . . . . . 224

Detailed Description of the Invention . . . . . . . . . 224

Drying of Spray by Moisture Removal . . . . . . 225

Separation of Dried Product from the Air . . 225

Ultimate Particle Size of the Feed . . . . . . . . . . 225

Concentration of Solids in the Feed . . . . . . . . 225

Viscosity and Temperature of the Feed . . . . . 226

Feed Rate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 226

Atomization of Feed into a Spray . . . . . . . . 226

Spray-Air Contact . . . . . . . . . . . . . . . . . . . . 226

Drying of Spray . . . . . . . . . . . . . . . . . . . . . . 226

There is disclosed a process for preparing superficially porous macroparticles comprising spray drying a

specified well-mixed slurry of core macroparticles, colloidal inorganic microparticles and a liquid, and sin-

tering the resulting product to cause a 5-30% decrease in surface area.