ABSTRACT

Sample Preparation . . . . . . . . . . . . . . . . . . . . . . . . . 891

Optical Microscopy . . . . . . . . . . . . . . . . . . . . . . . . . 892

Quantitative Image Analysis . . . . . . . . . . . . . . . . . . 892

Transmission Electron Microscopy and

Selected Area Electron Diffraction . . . . . . . . . . . . 892

Electron Probe X-Ray Microanalysis . . . . . . . . . . . 892

Modes of Analysis . . . . . . . . . . . . . . . . . . . . . . . . 892

ESCA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 893

Modes of Analysis . . . . . . . . . . . . . . . . . . . . . . . . 893

Scanning Auger Microanalysis . . . . . . . . . . . . . . . . 893

Modes of Analysis . . . . . . . . . . . . . . . . . . . . . . . . 893

X-Ray Diffraction . . . . . . . . . . . . . . . . . . . . . . . . . . 893

X-Ray Fluorescence . . . . . . . . . . . . . . . . . . . . . . . . . 893

Thermal Analysis (DSC, TGA) . . . . . . . . . . . . . . . . 893

Thermal Properties Which Can Be Measured . . 893

Thermo Nicolet Nexus/Continuum FTIR System . . 894 Scanning Electron Microscopy

and Energy Dispersive X-Ray Analysis . . . . . . . . 894

Modes of Analysis . . . . . . . . . . . . . . . . . . . . . . . . 894

Synopsis On Electron Beam/Solid Interactions To Characterize Samples . . . . . . . . . . . . . . . . . . . . . . . 894

Abbreviations . . . . . . . . . . . . . . . . . . . . . . . . . . . . 894

SEM and EPA . . . . . . . . . . . . . . . . . . . . . . . . . . . 894

Sample Preparation (General) . . . . . . . . . . . . . . . 895

Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 895

Acknowledgment . . . . . . . . . . . . . . . . . . . . . . . . . . . 895

The means for obtaining high quality, cost effective analytical services are described. These services are

essential for accurate and economical analysis with rapid turn around time. Good laboratory practices,

including computerized sample tracking, instrument calibration, maintenance of equipment and written

documentation of the analytical methods assure high quality of the analytical data.