ABSTRACT

Introduction ........................................................................................................ 525

Methodology....................................................................................................... 526

Results and Discussion ..................................................................................... 526

Conclusion .......................................................................................................... 529

Acknowledgments ............................................................................................. 529

References ........................................................................................................... 529

The complexity of the spray-drying process makes experimental study of

mass transfer in a real spray dryer impractical (Masters, 1985). Authors have

studied changes in moisture content of the material during the process by

suspending a drop of the liquid to be dried in a fixed position under an air

stream (Ferrari et al., 1989; Adhikari et al., 2000; Dolinsky, 2001). Droplet

diameter or particle size is a parameter of interest, but it is difficult to

estimate during drying given the many variables having an influence in the

spray-air contact stage. At the same time, phenomena related to

evaporation such as shrinkage, deformation, size increase, formation of

crust, and crush start to arise and will, in turn, influence actual heat and

mass transfer (McCormick, 1962; Chawla, 1994; Oakley, 1997). In spray-

drying processes, drying stages can be related to moisture evaporation and

morphology development of the particle (Kieviet and Kerhof, 1997; Oakley,

1997). Drying zones inside the chamber and change of moisture content

during dehydration may help to establish links between drier design and

product quality. An interesting option that would allow evaluation of the

height of drying stages inside the spray chamber is the application of the

concept of the heat transfer unit, which would represent an option and a

contribution to spray-drier design and operation. This method considers

that the longitude of the path that one of the fluids travels through the dryer

is formed by the number of transfer units (NtOG), which is a dimensionless

relationship between the difference of the temperature of the drying air and

the heat driving force. The height of the transfer unit (HtOG) is a function of

the airflow, overall heat transfer coefficient, and the heat capacity of drying

air. The product of the height of the heat transfer unit times the number of

transfer units is equal to the total height of the effective drying stages

(Masters, 1985).