ABSTRACT

By applying methods used by microscopists to the preparation of samples for infrared microspectroscopy, one can analyze particles less than 1 ng in size. For example, a dispersion of particles too small to analyze individually can be trans­ ferred to a KBr crystal and assembled to cover a larger area. Excellent spectra can be obtained for an array of 1-to 2-|mm particles by careful sample prepa­ ration. Techniques for solving similar problems have been carefully documented in this chapter. These techniques require practice and proper tools. These tech­ niques are extremely useful in isolating and identifying contaminants encoun­ tered in the pharmaceuticals, electronics, forensics, and manufacturing industries.