ABSTRACT

In this chapter to the Green Syntheses Series the reader is introduced to a number of example reactions taken from Organic Syntheses. Since reports appearing in this well-known and venerable series have their experimental procedures independently checked as a strict requirement for publication [1], it seems only tting that they would

Introduction .............................................................................................................. 13 Example 2.1: 1,3-Diphenyl-2-(1-Phenylethyl)-Propane-1,3-Dione ........................ 16 Example 2.2: 1-(4-Phenethyl-Phenyl)-Ethanone ..................................................... 21 Example 2.3: N-Benzyl-4-Phenyl-Butyramide ........................................................24 Example 2.4: Cyclen ................................................................................................29 Example 2.5: Dibenzyl-(1-Cyclohexyl-3-Trimethylsilanyl-Prop-2-ynyl)-Amine ... 33 Example 2.6: [2-(4-Fluoro-Phenyl)-1H-Indol-4-yl]-Pyrrolidin-1-yl-Methanone .... 33 Example 2.7: 3-Hydroxymethyl-4-Methyl-2-Methylene-Pentanoic Acid Methyl Ester .............................................................................................................36 Example 2.8: (3-Phenyl-Allyl)-Phosphinic Acid .....................................................36 Example 2.9: 9-Propionyl-3,4,5,8,9,10-Hexahydro-Oxecin-2-One ......................... 41 Example 2.10: 3a-Hydroxy-2,3-Diisopropoxy-4,6a-Dimethyl-4,5,6,6aTetrahydro-3aH-Pentalen-1-One .............................................................................. 41 Example 2.11: 7,7-Dimethyl-3-Phenyl-4-p-Tolyl-1,4,6,7,8,9-HexahydroPyrazolo[3,4-b]Quinolin-5-One ............................................................................... 42 References ................................................................................................................44