ABSTRACT

Murray [1] has described a gas chromatographic method for the determination in water of triarylphosphate esters (1mol S-140, tricresyl phosphate, cresol phosphate). These substances are used commercially as lubricant oil and plastic additives, hydraulic fluids and plasticizers. The method involves extraction from the samples, hydrolysis and measurement of the individual phenols by gas chromatography as the trimethylsilyl derivatives. The lower detection limit was about 3ppm.