ABSTRACT
Due to wide applications of NMR in chemistry, geochemistry, biochemistry, biology, etc., NMR experiments and the problems and solutions sought are quite varied. In spite of the standardization and development of NMR techniques and software, in some sense any complex NMR experiment and its interpretation can seem unique, particularly to inexperienced researchers who have dealt primarily with routine onedimensional (1D) and two-dimensional (2D) NMR spectra recorded for the analysis of reaction mixtures. Nevertheless, some problems require either the application of particular techniques and approaches or special knowledge and strategies. Some of these issues are considered in this chapter, the choice of which is obviously subjective.
