ABSTRACT

NMR spectroscopy has become a useful tool for chemical analysis of solids be­ cause control of spectral response allows one to analyze effects individually in separate experiments that would simultaneously be present in the usual NMR spectrum. I discuss in this chapter how one can obtain spectra of abundant nuclei such as protons or fluorines whose spectra are usually dominated by like-spin dipolar couplings and how one may analyze the spectrum of deuterium, a spin-1 nucleus whose dominant coupling in the solid state is the quadrupolar interaction with electric-field gradients [1-6].