ABSTRACT

Discussing the design and optimum use of thermal analysis instrumentation for materials' property measurement, this work details how the instruments work, what they measure, potential pitfalls and the fitting of experimental results to theoretical models. It presents a tutorial on writing computer programs for data manipulation, advanced thermoanal

chapter 1|2 pages

INTRODUCTION

chapter |2 pages

path

chapter |2 pages

the absolute zero in temperature.

chapter |2 pages

References

chapter 2|10 pages

FURNACES AND

TEMPERATURE MEASUREMENT

chapter 0|3 pages

04...--------------------.

chapter |8 pages

Semiconductor-Controlled Rectifiers

chapter |3 pages

that it overshoots the

chapter 3|10 pages

DIFFERENTIAL THERMAL ANALYSIS

chapter |9 pages

than per mole basis, it is

chapter |5 pages

than the

chapter |2 pages

at a constant value

chapter |6 pages

the heat flow due to the reaction

-------!'"""""'

chapter 4|2 pages

MANIPULATION OF DATA

chapter |2 pages

• • •

chapter 4|8 pages

2 Taking Derivatives of Experimental Data

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file ", file2$

chapter |2 pages

The plug-in

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Reference

chapter 5|22 pages

THERMOGRAVIMETRIC ANALYSIS

chapter 5|8 pages

. 3 . 4Discussion

chapter |1 pages

Chapter 6ADVANCEDAPPLICATIONS DTA

chapter |1 pages

herein-melting and first or-

chapter |2 pages

data set. By an iter-

chapter |1 pages

at a given time:

If at

chapter |10 pages

R is the gas constant

-Ea ) + Tr) dt

chapter |3 pages

k X

chapter 200000|2 pages

. ------------------,

chapter 7|1 pages

DILATOMETRY

INTERFEROMETRY

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...--------------..,..------,----,

chapter |1 pages

av lylz (a 8zTx) + (8 Ty) (azz)

+ 8T + + +

chapter 7|3 pages

. 2TheoreticalOrigins ThermalExpansion

chapter |3 pages

than

chapter |3 pages

( -b.l) ~ Q _+ l)

chapter |5 pages

the

chapter |13 pages

to as dispersion-toughened

chapter |1 pages

+-Laser

chapter |1 pages

References

chapter 8|4 pages

HEAT

PYROMETRY to Heat Transfer

chapter |8 pages

the shortest distances

chapter |1 pages

Disappearing Filament Pyrometry

chapter |5 pages

that is focused upon. External tungsten

chapter |5 pages

data to this func-

chapter |2 pages

References

chapter 9|4 pages

THERMAL CONDUCTIVITY

chapter 10|4 pages

VISCOSITY OF LIQUIDS

10.1 Background

chapter |2 pages

at a minimum. While the specimen volume remains con-

em\ v is the midpoint deflection rate (em/min),

chapter |2 pages

J. Stevens, and W. C

chapter |4 pages

Appendix A INSTRUMENTATION VENDORS

A.l Thermoanalytical Instrumentation

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Appendix SUPPLEMENTARYREADING

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of Interferometry, Academic Press,