ABSTRACT

Because of its simplicity of use and quantitative results, Scanning Electrochemical Microscopy (SECM) has become an indispensable tool for the study of surface reactivity. The fast expansion of the SECM field over several years has been fueled by the introduction of new probes, commercially available instrumentation, and new practical applications. Scanning Electrochemical Microscopy, Third Edition offers essential background and in-depth overviews of specific applications in self-contained chapters.

The vitality and growing popularity of SECM over the past 30+ years have largely been determined by its versatility and capability to remain useful in the changing scientific and technological environments. New applications reported during the last decade reflect significant current activity in biomedical and energy-related research. This thoroughly updated edition provides up-to-date comprehensive reviews of different aspects of SECM.

New chapters by renowned professionals in the field cover recent advances in different areas of SECM including nanoSECM, surface reactions and films, batteries, and fuel cells. Expanded coverage of electrocatalysis and surface interrogation as well as photoelectrochemistry and photoelectrocatalysis are also provided.

Useful for a broad range of interdisciplinary research—from biological systems to nanopatterning—this book is invaluable to all interested in learning and applying SECM.

chapter 1|10 pages

Introduction and Principles

ByAllen J. Bard

chapter 2|22 pages

Tip Preparation and Instrumentation for Nanoscale Scanning Electrochemical Microscopy

ByJiyeon Kim, Kevin C. Leonard

chapter 3|32 pages

Scanning Electrochemical Microscopic Imaging

ByKevin C. Leonard, Tess Seuferling, Jiyeon Kim, Fu-Ren F. Fan

chapter 4|40 pages

Theory

Edited ByMichael V. Mirkin, Yixian Wang

chapter 5|22 pages

Heterogeneous Electron-Transfer Reactions

ByShigeru Amemiya

chapter 6|28 pages

Electrocatalysis and Surface Interrogation

ByHyun S. Ahn, Cynthia G. Zoski, Allen J. Bard

chapter 7|26 pages

Nanoscale SECM

ByXiang Wang, Gaukhar Askarova, Michael V. Mirkin

chapter 8|26 pages

Molecular Transport in Membranes

ByMei Shen, Shigeru Amemiya

chapter 9|36 pages

Potentiometric Probes

ByGuy Denuault, Geza Nagy, Klara Tóth

chapter 10|54 pages

Biotechnological Application of Scanning Electrochemical Microscopy

ByBenjamin R. Horrocks, Gunther Wittstock

chapter 11|34 pages

Scanning Electrochemical Microscopy of Living Cells

ByChangyue Du, Thilini Suduwella, Isabelle Beaulieu, Steen B. Schougaard, Janine Mauzeroll

chapter 12|30 pages

Surface Reactions and Films

ByJean-Marc Noël, Philippe Hapiot

chapter 14|40 pages

Micro and Nanopatterning

Using Scanning Electrochemical Microscopy (SECM)
ByDaniel Mandler

chapter 15|62 pages

Micro and Nanopipettes for Electrochemical Imaging and Measurement

ByKristen Alanis, Sasha Elena Alden, Lane Allen Baker, Edappalil Satheesan Anupriya, Henry David Jetmore, Mei Shen

chapter 16|32 pages

Application to Batteries and Fuel Cells

ByZachary T. Gossage, Kendrich O. Hatfield, Yuanya Zhao, Raghuram Gaddam, Dipobrato Sarbapalli, Abhiroop Mishra, Joaquín Rodríguez-López

chapter 17|68 pages

Hybrid Scanning Electrochemical Techniques

Methods and Applications
ByChristine Kranz, Christophe Demaille

chapter 18|18 pages

Additional Recent Applications and Prospects

ByAndreas Lesch, Allen J. Bard, Hubert H. Girault