This volume provides a practical, intuitive approach to electroanalytical chemistry, presenting fundamental concepts and experimental techniques without the use of technical jargon or unnecessarily extensive mathematics. This edition offers new material on ways of preparing and using microelectrodes, the processes that govern the voltammetric behavior of microelectrodes, methods for characterizing chemically modified electrodes, electrochemical studies at reduced temperatures, and more. The authors cover such topics as analog instrumentation, overcoming solution resistance with stability and grace in potentiostatic circuits, conductivity and conductometry, electrochemical cells, carbon electrodes, film electrodes, microelectrodes, chemically modified electrodes, mercury electrodes, and solvents and supporting electrolytes.

chapter 1|9 pages

An Overview

ByPeter T. Kissinger

chapter 2|40 pages

Fundamental Concepts of Analytical Electrochemistry

ByPeter T. Kissinger, Carl R. Preddy, Ronald E. Shoup, William R. Heineman

chapter 3|75 pages

Large-Amplitude Controlled-Potential Techniques

ByWilliam R. Heineman, Peter T. Kissinger

chapter 4|13 pages

Large-Amplitude Controlled-Current Techniques

ByWilliam R. Heineman, Peter T. Kissinger

chapter 5|24 pages

Small-Amplitude Controlled-Potential Techniques

ByPeter T. Kissinger, Thomas H. Ridgway

chapter 6|30 pages

Introduction to Analog Instrumentation

ByPeter T. Kissinger

chapter 8|29 pages

Conductivity and Conductometry

ByF. James Holler, Christie G. Enke

chapter 9|25 pages

Electrochemical Cells

ByFred M. Hawkridge

chapter 10|40 pages

Carbon Electrodes

ByRichard L. McCreery, Kristin K. Cline

chapter 11|33 pages

Film Electrodes

ByJames L. Anderson, Nicholas Winograd

chapter 12|36 pages


ByAdrian C. Michael, R. Mark Wightman

chapter 13|40 pages

Chemically Modified Electrodes

ByCharles R. Martin

chapter 14|26 pages

Mercury Electrodes

ByZbigniew Galus

chapter 15|17 pages

Solvents and Supporting Electrolytes

ByAlbert J. Fry

chapter 16|24 pages

Electrochemical Studies at Reduced Temperature

ByDennis H. Evans

chapter 17|31 pages

Electroanalytical Chemistry in Molten Salts

ByCharles L. Hussey

chapter 18|25 pages

Vacuum-Line Techniques

ByVladimir Katovic

chapter 19|13 pages

Electrochemistry in the Dry Box

BySteven N. Frank

chapter 20|39 pages

Digital Simulation of Electrochemical Problems

ByJ. T. Maloy

chapter 21|18 pages

Evaluation of Mechanisms of Organic Reactions

ByM. Dale Hawley

chapter 22|41 pages

Electroorganic Synthesis

ByEberhard Steckhan

chapter 24|19 pages

Electrochemical Preconcentration

ByJoseph Wang

chapter 25|30 pages

Controlled-Current Coulometry

ByDavid J. Curran

chapter 26|44 pages

Electrochemistry in Pharmaceutical Analysis

ByMarvin A. Brooks, Eric W. Tsai

chapter 27|41 pages

Electrochemical Detection in Liquid Chromatography and Capillary Electrophoresis

BySusan M. Lunte, Craig E. Lunte, Peter T. Kissinger

chapter 28|45 pages

Photonic Electrochemistry

ByAndrew B. Bocarsly, Hiroyasu Tachikawa, Larry R. Faulkner

chapter 29|60 pages

Principles and Techniques of Electrochemical-Electron Paramagnetic Resonance Experiments

ByIra B. Goldberg, Ted M. McKinney