ABSTRACT

Damage and cyclic fatigue failure under alternating loading in transformation-toughened zirconia ceramics are reviewed and compared to corresponding behavior under quasi-static loading (static fatigue). Current understanding of the role of transformation toughening in influencing cyclic fatigue-crack propagation behavior is examined based on studies which altered the extent of the tetragonal-to-monoclinic phase transformation of Mg-PSZ through sub-eutectoid aging. These studies suggest that near-tip computations of the crack-driving force (in terms of the local stress intensity) can be used to predict crack-growth behavior under constant amplitude and variable-amplitude (spectrum) loading, using spatially resolved Raman spectroscopy to measure the extent of the transformation zones. In addition, results are reviewed which rationalize distinctions between the crack-growth behavior of pre-existing “long” (> 2 mm), through-thickness cracks and naturally-occurring, “small” (1 to 100 μm), surface cracks in terms of variations in crack-tip shielding with crack size. In the present study, the effect of grain size variations on crack-growth behavior under both monotonic (R-curve) and cyclic fatigue loading are examined. Such observations are used to speculate on the mechanisms associated with cyclic crack advance, involving such processes as alternating shear via transformation-band formation, cyclic modification of the degree of transformation toughening, and uncracked-ligament (or grain) bridging.