ABSTRACT

Freeze drying is accomplished by reducing the product

temperature so that most of the product moisture is in a

solid state, and by decreasing the pressure around the pro-

duct, sublimation of ice can be achieved.[1] Developments of

freeze drying owe much to advances in vacuum pumping

and refrigeration machines since the late 19th century. Yet

freeze drying had been regarded as an occasional scientific

tool until Flosdorf started his study on its industrial applica-

tions to food drying[2] and pharmaceutical drying[3] in

1930s. Since then, research and development in freeze dry-

ing of foods were promoted for military and commercial

purposes in the United States and several European coun-

tries, and then in the beginning of 1960s, these results,

including the process of accelerated freeze drying (AFD)

method,[4] were released to industry for commercial

PROCESS, EQUIPMENT, AND COSTS

Freeze Drying Process

Fig. 1 shows a typical freeze drying process for manufac-

turing an instant coffee, together with temperature profiles

of the product during the period of main freeze drying

operations: prefreezing, primary drying, and secondary

drying. It should be noted that all of them are not mechan-

ical, but thermal unit operations.