ABSTRACT

Introduction ........................................................................................................ 513

Materials and Methods ..................................................................................... 514

Results and Discussion ..................................................................................... 514

Conclusions......................................................................................................... 517

Acknowledgments ............................................................................................. 517

References ........................................................................................................... 517

In spray drying, inadequate drying conditions can produce a powder with

nondesirable characteristics. The size distribution of the droplets is the

variable that influences most the properties of final products. Droplet

diameter or particle size is a very important parameter but difficult to

evaluate given the many variables influencing it (Furuta et al., 1994; Kieviet

and Kerhof, 1997; Aguilera and Stanley, 1999; Chanona et al., 2003). At the

same time, phenomena associated with evaporation such as shrinkage,

deformation, expansion, formation of crust, and breakage arise (Liang and

King, 1991; Oakley, 1997; Walton, 2000). The thickness of the crust will

depend on drying velocity. High drying rates tend to produce large particles

with a thin crust and low density, whereas low drying velocity produces

small particles with a thick crust and high density (Masters, 1985; Oakley,

1997). Also, depending on the temperature of the particles, the liquid caught

inside may vaporize and generate pressure. If a portion of the crust is

broken, water vapor will be displaced and hollow spheres or fragments of

spheres will be produced, which may improve rehydration. If the crust is

flexible, particles may expand or collapse depending on drying conditions

(Oakley, 1997; Walton, 2000).