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      Chapter

      ◾ Characterization Methods for Studying Nanomaterials
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      Chapter

      ◾ Characterization Methods for Studying Nanomaterials

      DOI link for ◾ Characterization Methods for Studying Nanomaterials

      ◾ Characterization Methods for Studying Nanomaterials book

      ◾ Characterization Methods for Studying Nanomaterials

      DOI link for ◾ Characterization Methods for Studying Nanomaterials

      ◾ Characterization Methods for Studying Nanomaterials book

      ByGerrard Eddy Jai Poinern
      BookA Laboratory Course in Nanoscience and Nanotechnology

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      Edition 1st Edition
      First Published 2014
      Imprint CRC Press
      Pages 24
      eBook ISBN 9780429173677
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      ABSTRACT

      During the beam-surface interaction, several mechanisms take place, such as those involving secondary electrons (SEs), backscattered electrons (BSEs), and X-rays, as shown in Figure 3.1b(ii). SEs are ejected from the sample aer colliding with atoms in the upper layers of the surface and are collected by the SE detector and used for imaging the surface topography. In addition to the emission of SEs are the BSEs, which are detected using a solid-state detector (Everhart-ornley detector). e intensity of BSE is dependent on the atomic number of the sample material, accelerating voltage, and interaction volume. Importantly, the BSEs are used to create compositional maps of the specimen. However, because the interaction volume is greater for BSEs, the resolution is usually of lower quality than those of SEs. In addition to the SEs and BSEs, the SEM also produces characteristic X-rays, which can be used to determine the elements present in the sample material. erefore, by scanning the sample surface topographical features and composition, data can be viewed, stored, or recorded as a micrograph.

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